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Monday, September 23, 2019

The reason for the QuEChERS matrix effect in the liquid state is generally considered to be due to the non-volatile components in the matrix and the substance to be tested, which competes in the ionization process. The matrix effect in gas phase temperament is generally attributed...

Friday, September 20, 2019

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Friday, September 20, 2019

Silica matrix HPLC columns are generally compatible, but organic polymer matrix columns may expand or contract in some solvent combinations, which will affect their chromatographic behavior. Wash each solvent system at least 20 volumes. Because some solvent systems are highly viscous...

Friday, September 20, 2019

Solid phase extraction is essentially a liquid chromatographic separation. The main separation mode is the same as that of liquid chromatography. It can be divided into normal phase (the polarity of the adsorbent is greater than the polarity of the eluent), and the reverse phase (the...)

Wednesday, September 18, 2019

Selection of scavengers The conventional QuEChERS method only uses PSA which is too simple single that can no longer meet the complex matrix samples examination experiments. GCB (graphitized carbon black) can effectively adsorb pigments, non-polar interferences such as sterol due...

Monday, September 16, 2019

Reversed phase chromatography (RP) is the most widely used technique in high-performance liquid chromatography (HPLC) up to now, mainly because it is suitable for the analysis of most of them. Nonpolar substances and many ionizable and ionic compounds. Most stationary phases used...

Wednesday, September 11, 2019

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Wednesday, September 11, 2019

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Tuesday, September 10, 2019

1. Advantages and disadvantages of commonly used extraction solvents Acetonitrile: easy to salt out; compatible with LC/MS; difficult to concentrate Acetone: not easy to salt out; easy to volatilize, concentrate Ethyl acetate: immiscible with water; less extraction of impurities;...

Tuesday, September 03, 2019

The basic principle of SPE cartridges is that the liquid sample is made to pass through the adsorbent to retain the tested substance, and then the impurities are washed away with appropriate strength solvent, and then the tested substance is eluted with a small amount of good solvent...

Friday, August 30, 2019

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Friday, August 30, 2019

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Friday, August 16, 2019

NH2 HPLC columns refer to the chromatographic columns that use silica gel as matrix carrier to bond amino groups. They are usually used for the analysis of carbohydrate compounds, and the mobile phase is usually methanol, acetonitrile and buffers salt solution. - The cleaning method...

Friday, August 16, 2019

- Category - In terms of the filler type, SPE column can be divided into four applications of silicone bonding matrix, polymer matrix, absorption matrix and specialized columns. Besides, the silicone bonding has four sorts—antiphase(C18 sealing end/uncapped/hydrophile, C8), positive...

Thursday, August 15, 2019

Review the article that I had written for product introductions, it seems that the content which making fun of products basically does not have, a person with the label of “warm person heart” is wearing very tired. The things about making fun are so cool to be said completely by naked...

Wednesday, August 14, 2019

After years of development, the QuEChERS pretreatme nt method has been continuously improved and broadened by researchers as a simple and rapid residual pretreatment technology. The application target also has been extended from the highest moisture content of vegetables and fruits...

Wednesday, August 14, 2019

The important technical parameters of Hawach SPE Columns are the key points of selection. Material The material selection of the SPE column is very important. The column material is in direct contact with the test object or analyte. The quality of material selection determines the...

Monday, August 12, 2019

Solid phase extraction principle Solid phase extraction is a separation technique that combines selective retention, selective elution, and the like. When a complex sample solution passes through the sorbent, the sorbent selectively retains the aimed compound and a small number of...

Thursday, August 08, 2019

Most common SPE cartridges are injection syringes made of polyethylene, in which there are two plugs made of polypropylene or fiberglass, with a certain amount of chromatographic adsorbent (filler) between the two plugs. SPE cartridges without sieve plate 1. Avoid “non-specific adsorption” 2...

Wednesday, August 07, 2019

Food safety testing is a major issue related to people's livelihood. In recent years, the QuEChERS method has been widely used in the pretreatment of food safety detection samples. In addition, the method has been applied to trace analysis. QuEChERS Application The international application...

Tuesday, August 06, 2019

Ion-exchange solid phase extraction is widely used in biological samples and environmental monitoring. During the extraction process, the pH of the sample is adjusted so that the solute is easily ionized. The solute is exchanged from the resin by changing the pH or increasing the...

Thursday, August 01, 2019

There are two different cases of retention time: retention time drift and retention time fluctuations. The former means that the retention time changes only in one direction, while the latter refers to the fluctuation of the retention time without a fixed law. It is often helpful...

Tuesday, July 30, 2019

Since its birth, the QuEChERS method has been widely used in pesticide residue analysis due to its unique advantages and characteristics of fast, simple and cheap. Lehotay et al. established a method, which uses the QuEChERS method to treat samples and analyze 229 kinds of pesticides...

Friday, July 19, 2019

Bonded-phase chromatography is a liquid-liquid chromatography method in which a stationary phase is covalently bound to a carrier particle, which overcomes the mechanical shock in the distribution chromatography, the constant loss of the stationary phase and the gradual change of...

Friday, July 12, 2019

Today, Hawach want to talk about the pre-treatment process for pesticide residue detection from the perspective of food safety – QuEChERS, and also tell you how to pre-treat pesticide residue food. Introduction The present analytical methods and determining techniques, pre-treatment...

Thursday, July 11, 2019

With the development of society and technology, chromatographic analysis theory has also been developing rapidly. HPLC column has now been widely applied in every field of laboratory analysis. HPLC column gathers function of both detection and separation. With the right choice, use...

Thursday, July 11, 2019

With the development of society and technology, chromatographic analysis theory has also been developing rapidly. HPLC column has now been widely applied in every field of laboratory analysis. HPLC column gathers function of both detection and separation. With the right choice, use...

Tuesday, July 09, 2019

Polymeric MCX SPE cartridges are used to extract strongly alkaline compounds. MCX is a mixed strong cation exchange adsorbent obtained by bonding sulfonic acid groups on highly crosslinked PS/DVB surface. It has both reverse phase and cationic exchange retentive properties and good...

Tuesday, July 02, 2019

The average sample addition recovery rate of QuEChERS method is higher than 85%, with fewer impurities interfering with the detection of the target substance, a small amount of solvent, simple and fast operation, which will be the preferred pretreatment method for routine detection...

Monday, June 24, 2019

QuEChERS is widely used in many areas, in the case that the targeting recovery rate satisfies the need, and also the matrix background of removing impurities meets detection, it can be applied to purify stuff such as residues of food and veterinary, additives, plasticizers. However...